(E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

Base Information

Chemical Name:(E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid
CAS No.:923978-71-6
Molecular Formula:C₂₀H₂₀O₄S
Molecular Weight:356.442
Hs Code.:

Synonyms:(E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

Suppliers and Price of (E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

There total 4 articles about (E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: C₂₂H₂₄O₄S

: 923978-71-6
(E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 50 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2021.113417

Reference yield:

: (2E)-3-(4-hydroxy-3,5-dimethylphenyl)-1-[4-(methylsulfanyl)phenyl]prop-2-en-1-one

: 923978-71-6
(E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 90 °C / Inert atmosphere

2: lithium hydroxide; water / tetrahydrofuran / 50 °C / Inert atmosphere

With water; potassium carbonate; lithium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2021.113417

Reference yield:

: 1778-09-2
4-(Methylthio)acetophenone

: 923978-71-6
(E)-2-(2,6-dimethyl-4-(3-(4-(methylthio)phenyl)-3-oxoprop-1-en-1-yl)phenoxy)acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol / 24 h / 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 6 h / 90 °C / Inert atmosphere

3: lithium hydroxide; water / tetrahydrofuran / 50 °C / Inert atmosphere

With hydrogenchloride; water; potassium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2021.113417