2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole

Base Information

Chemical Name:2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole
CAS No.:1012330-31-2
Molecular Formula:C₂₄H₃₀INO₃Si
Molecular Weight:535.497
Hs Code.:

Synonyms:2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole

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Chemical Property of 2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole

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Technology Process of 2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole

There total 1 articles about 2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1012330-29-8
2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)oxazole

: 1012330-31-2
2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole

Guidance literature:: 2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)oxazole; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 2h;

With iodine; In tetrahydrofuran; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jm701210y

Reference yield: 97.0%

: 1012330-31-2
2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole

: 1012330-32-3
1-(5-iodooxazol-2-yl)-3-(4-phenoxyphenyl)propan-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1021/jm701210y

Reference yield: 80.0%

: 1012330-31-2
2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-iodooxazole

: 680-15-9
2,2-difluoro-2-(fluorosulfonyl)acetate

: 1012330-33-4
2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-(trifluoromethyl)oxazole

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; In N,N-dimethyl-formamide; at 70 ℃; for 2.5h;
DOI:10.1021/jm701210y