2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide

Base Information

• Chemical Name: 2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide
• CAS No.: 1391748-77-8
• Molecular Formula: C₃₆H₄₈N₄O₄
• Molecular Weight: 600.802

Synonyms:2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide

Chemical Property of 2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide

Chemical Property:

Purity/Quality:

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Technology Process of 2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide

There total 2 articles about 2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-phenyl-propionaldehyde (104-53-0) → 2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide (1391748-77-8)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / 24 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In methanol; ethanol;

DOI:10.1002/anie.201200822

Reference yield:

C27H37N3O2 → 2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide (1391748-77-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 50 °C / Inert atmosphere

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In methanol; ethanol;

DOI:10.1002/anie.201200822

Reference yield: 97.0%

2,2-dimethyl-N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N-[2-(3-phenylpropylamino)ethyl]propionamide (1391748-77-8) → N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N'-(3-phenylpropyl)ethane-1,2-diamine (1391748-68-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h;

DOI:10.1002/anie.201200822

upstream raw materials:

3-phenyl-propionaldehyde

Downstream raw materials:

N-{2-[[2-(4-nitrophenyl)allyl]-(3-phenylpropyl)amino]ethyl}-N'-(3-phenylpropyl)ethane-1,2-diamine

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