N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Base Information

Chemical Name:N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine
CAS No.:1558010-20-0
Molecular Formula:C₄₇H₃₆N₄O₂S
Molecular Weight:720.894
Hs Code.:

Synonyms:N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

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Chemical Property of N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

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Technology Process of N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

There total 5 articles about N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1558010-19-7
N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

: 670-54-2
ethenetetracarbonitrile

: 1558010-20-0
N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Guidance literature:: In N,N-dimethyl-formamide; at 140 ℃; for 6h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2013.12.079

Reference yield:

: 1558010-18-6
2-(2-bromo-9,10-dipropoxyanthracen-6-yl)thiophene

: 1558010-20-0
N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 24 h / Inert atmosphere; Reflux

2: N,N-dimethyl-formamide / 6 h / 140 °C / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; N,N-dimethyl-formamide; toluene; 1: |Suzuki Coupling;
DOI:10.1016/j.tet.2013.12.079

Reference yield:

: 131-14-6,168681-29-6
2,6-diamino-9,10-anthraquinone

: 1558010-20-0
N-(phenyl-4-ethene-1,2,2-tricarbonitrile)-N-phenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Guidance literature:: Multi-step reaction with 5 steps

1: t-butylnitrite; copper(ll) bromide / acetonitrile

2: sodium disulfite; sodium hydroxide / water; dichloromethane

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 16 h / Reflux; Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 24 h / Inert atmosphere; Reflux

5: N,N-dimethyl-formamide / 6 h / 140 °C / Inert atmosphere; Reflux

With sodium disulfite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butylnitrite; potassium carbonate; sodium hydroxide; copper(ll) bromide; In dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 3: |Stille Cross Coupling / 4: |Suzuki Coupling;
DOI:10.1016/j.tet.2013.12.079