N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Base Information

Chemical Name:N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine
CAS No.:1558010-19-7
Molecular Formula:C₄₂H₃₇NO₂S
Molecular Weight:619.827
Hs Code.:

Synonyms:N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

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Technology Process of N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

There total 4 articles about N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1558010-18-6
2-(2-bromo-9,10-dipropoxyanthracen-6-yl)thiophene

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1558010-19-7
N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2013.12.079

Reference yield:

: 131-14-6,168681-29-6
2,6-diamino-9,10-anthraquinone

: 1558010-19-7
N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Guidance literature:: Multi-step reaction with 4 steps

1: t-butylnitrite; copper(ll) bromide / acetonitrile

2: sodium disulfite; sodium hydroxide / water; dichloromethane

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 16 h / Reflux; Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 24 h / Inert atmosphere; Reflux

With sodium disulfite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; t-butylnitrite; potassium carbonate; sodium hydroxide; copper(ll) bromide; In dichloromethane; water; toluene; acetonitrile; 3: |Stille Cross Coupling / 4: |Suzuki Coupling;
DOI:10.1016/j.tet.2013.12.079

Reference yield:

: 844696-83-9
2,6-dibromo-9,10-dipropoxyanthracene

: 1558010-19-7
N,N-diphenyl-4-(9,10-dipropoxy-2-(thiophen-2-yl)anthracen-6-yl)benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 16 h / Reflux; Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; water / 24 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; 1: |Stille Cross Coupling / 2: |Suzuki Coupling;
DOI:10.1016/j.tet.2013.12.079