methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate

Base Information

Chemical Name:methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate
CAS No.:1146510-34-0
Molecular Formula:C₂₁H₂₀O₆
Molecular Weight:368.386
Hs Code.:

Synonyms:methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate

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Chemical Property of methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate

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Technology Process of methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate

There total 1 articles about methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 15206-55-0
methyl 2-oxo-2-phenylacetate

: 516-09-6
4-hydroxy-3-methyl-5H-furan-2-one

: 1146510-34-0
methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate

Guidance literature:: 4-hydroxy-3-methyl-5H-furan-2-one; With n-butyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃;

methyl 2-oxo-2-phenylacetate; In tetrahydrofuran; hexane; at -78 - 20 ℃;

In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/jm801500h

Reference yield: 48.0%

: 1146510-34-0
methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate

: 1350907-84-4
methyl 2-(3-hydroxy-4-methyl-5-oxofuran-2(5H)-ylidene)-2-phenylacetate

Guidance literature:: With 1% Pd/C; hydrogen; In dichloromethane; at 20 ℃;
DOI:10.1021/jm801500h

Reference yield: 18.0%

: 1146510-34-0
methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate

: methyl 2-(3-(benzyloxy)-4-methyl-5-oxofuran-2(5H)-ylidene)-2-phenylacetate

Guidance literature:: methyl 2-(3-(benzyloxy)-4-methyl-5-oxo-2.5-dihydrofuran-2-yl)-2-hydroxy-2-phenyl acetate; With dmap; triethylamine; trifluoroacetic anhydride; In dichloromethane; at 0 - 20 ℃; for 12h;

With hydrogenchloride; In dichloromethane; water;
DOI:10.1021/jm801500h