(1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione

Base Information

• Chemical Name: (1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione
• CAS No.: 330160-19-5
• Molecular Formula: C₂₈H₂₈N₂O₂
• Molecular Weight: 424.543

Synonyms:(1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione

Chemical Property of (1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione

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Technology Process of (1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione

There total 1 articles about (1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

α,α'-dibromo-o-xylene (91-13-4) + 1,4-N,N-[(S)-1-phenylethyl]-piperazine-2,5-dione (158547-56-9) → (1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.03,8]tetradeca-3,5,7-triene-12,14-dione (330160-19-5)

Guidance literature:

1,4-N,N-[(S)-1-phenylethyl]-piperazine-2,5-dione; With lithium hexamethyldisilazane; In tetrahydrofuran; at -10 ℃; for 1h;

α,α'-dibromo-o-xylene; In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.1016/S0957-4166(00)00450-X

Reference yield: 94.0%

(1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.03,8]tetradeca-3,5,7-triene-12,14-dione (330160-19-5) + methyl iodide (74-88-4) → (1S,10S,1'S)-11,13-bis-[N-(1'-phenethyl)]-1-methyl-11,13-diazatricyclo[8.2.2.03,8]tetradeca-3,5,7-triene-12,14-dione

Guidance literature:

(1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione; With methyllithium; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

methyl iodide; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1016/S0957-4166(02)00262-8

Reference yield: 87.0%

bromethyl methyl ether (13057-17-5) + (1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.03,8]tetradeca-3,5,7-triene-12,14-dione (330160-19-5) → (1R,10S,1'S)-11,13-bis-[N-(1'-phenethyl)]-1-methoxymethyl-11,13-diazatricyclo[8.2.2.03,8]tetradeca-3,5,7-triene-12,14-dione

Guidance literature:

(1S,10S,1'S)-11,13-bis-[N,N-(1'-phenethyl)]-11,13-diazatricyclo[8.2.2.0^3,8]tetradeca-3,5,7-triene-12,14-dione; With methyllithium; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

bromethyl methyl ether; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1016/S0957-4166(02)00262-8

upstream raw materials:

α,α'-dibromo-o-xylene

1,4-N,N-[(S)-1-phenylethyl]-piperazine-2,5-dione

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