Technology Process of C47H55F6NO13S2
There total 6 articles about C47H55F6NO13S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide;
In
tetrahydrofuran; methanol; water;
at 0 - 50 ℃;
for 1h;
Inert atmosphere;
DOI:10.1039/c3cc42852d
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium hydroxide / methanol; water / 12 h / 0 - 20 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
3: lithium hydroxide / methanol; water; tetrahydrofuran / 1 h / 0 - 50 °C / Inert atmosphere
With
ammonium hydroxide; potassium carbonate; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42852d
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 100 °C / Inert atmosphere
2: lithium hydroxide / methanol; water; tetrahydrofuran / 1 h / 0 - 50 °C / Inert atmosphere
With
potassium carbonate; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42852d