6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside
CAS No.:117703-05-6
Molecular Formula:C₄₃H₅₁NO₉
Molecular Weight:725.879
Hs Code.:

Synonyms:6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Chemical Property of 6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Technology Process of 6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 5 articles about 6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 16697-49-7
3,4,6-tri-O-benzyl-1,2-O-(methoxyethylidene)-β-D-mannopyranose

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 117703-05-6
6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: With mercury dibromide; In acetonitrile; for 1.16667h; Heating;

Reference yield:

: 3254-16-8,4435-05-6,19189-54-9,29748-21-8,50801-29-1,64727-26-0,64727-27-1,65338-02-5,67672-68-8,78418-55-0,80877-03-8,103002-27-3,103002-29-5,132562-62-0
3,4,6-tri-O-acetyl-1,2-O-(1-methoxyethylidene)-β-D-mannopyranose

: 117703-05-6
6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NH₃ in MeOH (sat.), 2) NaH / 1) 48 h, RT, 2) DMF, 3) DMF, 18 h, RT

2: 45 percent / HgBr₂ / acetonitrile / 1.17 h / Heating

With ammonia; sodium hydride; mercury dibromide; In acetonitrile;

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 117703-05-6
6-(N-benzyloxycarbonylamino)-hexyl-2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 1N NaOH / tetrahydrofuran / 4 °C

2: 45 percent / HgBr₂ / acetonitrile / 1.17 h / Heating

With sodium hydroxide; mercury dibromide; In tetrahydrofuran; acetonitrile;