4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

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Chemical Name:4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)
CAS No.:109304-42-9
Molecular Formula:C₆₉H₉₄NO₁₂P
Molecular Weight:1160.48
Hs Code.:

Synonyms:4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

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Chemical Property of 4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

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Technology Process of 4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

There total 8 articles about 4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 87357-67-3
(R)-3-benzyloxytetradecanoic acid

: 109304-43-0
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

: 109304-42-9
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; at 4 ℃;
DOI:10.1016/0008-6215(87)80202-1

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 109304-42-9
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-p-sulfonic acid monohydrate / dimethylformamide / 3 h / 55 - 60 °C

2: 82.7 percent / buthyl-lithium / benzene; hexane / 0.17 h / -70 °C

3: 86 percent / dicyclohexylcarbodi-imide / 4-dimethylaminopyridine / 4 °C

With n-butyllithium; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; dmap; In hexane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0008-6215(87)80202-1

Reference yield:

: 538-60-3
dibenzyl hydrogen phosphite

: 109304-42-9
4,6-O-benzylidene-2-<(R)-3-benzyloxytetradecanamido>-3-O-<(R)-3-benzyloxytetradecanoyl>-2-deoxy-α-D-glucopyranose 1-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 3 steps

1: N-chlorosuccinimide / benzene / 1 h

2: 82.7 percent / buthyl-lithium / benzene; hexane / 0.17 h / -70 °C

3: 86 percent / dicyclohexylcarbodi-imide / 4-dimethylaminopyridine / 4 °C

With N-chloro-succinimide; n-butyllithium; dicyclohexyl-carbodiimide; dmap; In hexane; benzene;
DOI:10.1016/0008-6215(87)80202-1