N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide

Base Information

Chemical Name:N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide
CAS No.:1012865-68-7
Molecular Formula:C₂₅H₃₉IN₂O₃SSi
Molecular Weight:602.652
Hs Code.:

Synonyms:N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide

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Chemical Property of N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide

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Technology Process of N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide

There total 1 articles about N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 888703-23-9
C₂₅H₄₀N₂O₄SSi

: 1012865-68-7
N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 25 ℃; for 16h;
DOI:10.1016/j.bmcl.2007.08.040

Reference yield: 78.0%

: 887969-56-4
C₁₆H₂₂BrNO₄

: 1012865-68-7
N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide

: 888703-24-0
C₄₁H₆₁N₃O₇SSi

Guidance literature:: N-[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)-6-(5-iodo-3-phenylpentyl)pyridin-2-yl]-N-methylmethanesulfonamide; With zinc; In tetrahydrofuran; at 25 ℃; for 3h;

C₁₆H₂₂BrNO₄; [(t-Bu)3P]2Pd; In tetrahydrofuran; at 75 ℃; for 16h; Further stages.;
DOI:10.1016/j.bmcl.2007.08.040