α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative

Base Information

Chemical Name:α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative
CAS No.:81440-38-2
Molecular Formula:C₅₀H₄₆N₄O₁₀S₂
Molecular Weight:927.068
Hs Code.:

Synonyms:α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative

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Chemical Property of α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative

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Technology Process of α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative

There total 1 articles about α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 75626-73-2
benzyl (-)-(R)-4-chloro-4-oxo-2-<<(benzyloxy)carbonyl>amino>butyrate

: 1141-88-4
2-Aminophenyl disulfide

: 81440-38-2
α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative

Guidance literature:: With N-ethyl-N,N-diisopropylamine; at 4 ℃; for 4h;
DOI:10.1021/jm00369a016

Reference yield:

: 81440-38-2
α-benzyl N-(benzyloxycarbonyl)-D-aspartate o-mercaptoanilide, disulfide derivative

: (R)-3-Benzothiazol-2-yl-2-benzyloxycarbonylamino-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Zn, glacial AcOH / 50 °C

2: Et₃N / dioxane / Ambient temperature; pH 10

3: H₂, glacial AcOH / 10percent Pd/C / 4 h / 760 Torr

With hydrogen; acetic acid; triethylamine; zinc; palladium on activated charcoal; In 1,4-dioxane;
DOI:10.1021/jm00369a016