2-(benzyloxycarbonylamino)-2-ethylmalonic acid

Base Information

Chemical Name:2-(benzyloxycarbonylamino)-2-ethylmalonic acid
CAS No.:1395360-84-5
Molecular Formula:C₁₃H₁₅NO₆
Molecular Weight:281.265
Hs Code.:

Synonyms:2-(benzyloxycarbonylamino)-2-ethylmalonic acid

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Chemical Property of 2-(benzyloxycarbonylamino)-2-ethylmalonic acid

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Technology Process of 2-(benzyloxycarbonylamino)-2-ethylmalonic acid

There total 3 articles about 2-(benzyloxycarbonylamino)-2-ethylmalonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1395360-80-1
diethyl 2-(benzyloxycarbonylamino)-2-ethylmalonate

: 1395360-84-5
2-(benzyloxycarbonylamino)-2-ethylmalonic acid

Guidance literature:: diethyl 2-(benzyloxycarbonylamino)-2-ethylmalonate; With water; sodium hydroxide; In ethanol; at 20 ℃; for 96h;

With hydrogenchloride; water; In ethanol; Cooling with ice;
DOI:10.1055/s-0031-1290974

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1395360-84-5
2-(benzyloxycarbonylamino)-2-ethylmalonic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / water / 20 °C / Cooling with ice

2.1: sodium ethanolate / ethanol / 10 h / 87 °C

3.1: water; sodium hydroxide / ethanol / 96 h / 20 °C

3.2: Cooling with ice

With water; sodium ethanolate; sodium carbonate; sodium hydroxide; In ethanol; water;
DOI:10.1055/s-0031-1290974

Reference yield:

: 3005-66-1
diethyl 2-benzyloxycarbonylaminomalonate

: 1395360-84-5
2-(benzyloxycarbonylamino)-2-ethylmalonic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / ethanol / 10 h / 87 °C

2.1: water; sodium hydroxide / ethanol / 96 h / 20 °C

2.2: Cooling with ice

With water; sodium ethanolate; sodium hydroxide; In ethanol;
DOI:10.1055/s-0031-1290974