4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione

Base Information

• Chemical Name: 4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione
• CAS No.: 60598-01-8
• Molecular Formula: C₂₈H₃₈N₄O₈S₂
• Molecular Weight: 622.764

Synonyms:4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione

Chemical Property of 4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione

Chemical Property:

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Technology Process of 4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione

There total 2 articles about 4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,6-ditosyl-3,6-diazaoctanedioyl dichloride (39678-05-2) + diaza[12]crown-4 (294-92-8) → 4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione (60598-01-8)

Guidance literature:

With triethylamine;

DOI:10.1002/hlca.19760590516

Reference yield:

→ 4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione (60598-01-8)

Guidance literature:

Reference yield:

4,7-bis-(toluene-4-sulfonyl)-13,18-dioxa-1,4,7,10-tetraaza-bicyclo[8.5.5]eicosane-2,9-dione (60598-01-8) → 4,7-bis(p-tolylsulphonyl)-13,18-dioxa-1,4,7,10-tetra-azabicyclo<8,5,5>icosane (60598-02-9)

Guidance literature:

With borane-THF;

DOI:10.1002/hlca.19760590516

upstream raw materials:

3,6-ditosyl-3,6-diazaoctanedioyl dichloride

diaza[12]crown-4

Downstream raw materials:

4,7-bis(p-tolylsulphonyl)-13,18-dioxa-1,4,7,10-tetra-azabicyclo<8,5,5>icosane

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