propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside
CAS No.:191925-35-6
Molecular Formula:C₂₅H₃₃NO₅
Molecular Weight:427.541
Hs Code.:

Synonyms:propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

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Chemical Property of propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

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Technology Process of propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

There total 5 articles about propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 191925-32-3
allyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

: 191925-35-6
propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 100 ℃; for 2h;
DOI:10.1016/S0008-6215(97)00039-6

Reference yield:

: 100-52-7
benzaldehyde

: 191925-35-6
propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / Heating

2: 4.0 g / sodium borohydride / methanol / 1.5 h / 0 °C

3: 90 percent / sodium borohydride / 3 h

4: 90 percent / potassium t-butoxide / dimethylsulfoxide / 2 h / 100 °C

With sodium tetrahydroborate; potassium tert-butylate; In methanol; dimethyl sulfoxide; benzene; 1: Condensation / 2: Reduction / 3: Reduction / 4: Isomerization;
DOI:10.1016/S0008-6215(97)00039-6

Reference yield:

: 191925-27-6
allyl 2-amino-6-O-benzyl-2-deoxy-α-D-glucopyranoside

: 191925-35-6
propenyl 6-O-benzyl-2-(N-benzyl-N-ethyl)amino-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: benzene / Heating

2: 4.0 g / sodium borohydride / methanol / 1.5 h / 0 °C

3: 90 percent / sodium borohydride / 3 h

4: 90 percent / potassium t-butoxide / dimethylsulfoxide / 2 h / 100 °C

With sodium tetrahydroborate; potassium tert-butylate; In methanol; dimethyl sulfoxide; benzene; 1: Condensation / 2: Reduction / 3: Reduction / 4: Isomerization;
DOI:10.1016/S0008-6215(97)00039-6