ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside

Base Information

• Chemical Name: ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside
• CAS No.: 1009630-68-5
• Molecular Formula: C₂₃H₂₈O₆S
• Molecular Weight: 432.538

Synonyms:ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside

Chemical Property of ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside

Chemical Property:

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Technology Process of ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside

There total 2 articles about ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C26H32O6S (1009630-66-3) → ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside (1009630-68-5)

Guidance literature:

With 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; at 40 ℃;

DOI:10.1055/s-2007-992352

Reference yield: 83.0%

p-methoxybenzyl chloride (824-94-2) + ethyl (S)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside (131564-36-8) → ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside (1009630-68-5)

Guidance literature:

ethyl (S)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside; With di(n-butyl)tin oxide; In toluene; for 6h; Reflux; Dean-Stark;

p-methoxybenzyl chloride; With cesium fluoride; In N,N-dimethyl-formamide; at 70 ℃; for 12h; Dean-Stark;

DOI:10.1039/c5ra00759c

Reference yield: 89.0%

ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside (1009630-68-5) + benzyl bromide (100-39-0) → ethyl 2-O-benzoyl-3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside (1187765-97-4)

Guidance literature:

ethyl 3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

benzyl bromide; In N,N-dimethyl-formamide; at 0 ℃; for 2h;

DOI:10.1002/chem.201203865

upstream raw materials:

C₂₆H₃₂O₆S

p-methoxybenzyl chloride

ethyl (S)-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

Downstream raw materials:

ethyl 2-O-benzoyl-3-O-(para-methoxyphenyl)methyl-4:6-O-phenylmethylene-1-thio-β-D-galactopyranoside

2,6-dimethylphenyl (2-O-benzyl-4,6-O-benzylidene-3-O-chloroacetyl-α-D-galactopyranosyl)-(1→4)-1-thio-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranoside

2-O-benzyl-4,6-O-benzylidene-3-O-chloroacetyl-α-D-galactopyranose

2-O-benzyl-4,6-O-benzylidene-3-O-chloroacetyl-β-D-galactopyranose

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