2-bromo-1-salicylideneaminoethane

Base Information

• Chemical Name: 2-bromo-1-salicylideneaminoethane
• CAS No.: 80622-20-4
• Molecular Formula: C₉H₁₀BrNO
• Molecular Weight: 228.088
• Mol file: 80622-20-4.mol

Synonyms:2-bromo-1-salicylideneaminoethane

Chemical Property of 2-bromo-1-salicylideneaminoethane

Chemical Property:

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Technology Process of 2-bromo-1-salicylideneaminoethane

There total 1 articles about 2-bromo-1-salicylideneaminoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-bromoethylamine hydrobromide (2576-47-8) + salicylaldehyde (90-02-8) → 2-bromo-1-salicylideneaminoethane (80622-20-4)

Guidance literature:

With sodium hydroxide; In ethanol; water; for 4h; Reflux;

DOI:10.1016/j.poly.2011.09.011

Reference yield: 98.0%

1-benzylimidazole (4238-71-5) + 2-[2-bromoethyliminomethyl]phenol (80622-20-4) → C19H20N3O(1+)*Br(1-)

Guidance literature:

In neat (no solvent); at 60 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.ica.2018.09.057

Reference yield: 98.0%

2-[2-bromoethyliminomethyl]phenol (80622-20-4) + 2-[(1H-imidazol-1-yl)methyl]pyridine (62154-62-5) → C18H19N4O(1+)*Br(1-)

Guidance literature:

at 60 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

DOI:10.1080/00958972.2018.1493199

upstream raw materials:

2-bromoethylamine hydrobromide

salicylaldehyde

Downstream raw materials:

1,4-bis(2-salicylideneaminoethyl)piperazine

salicylaldehyde

N,N'-ethylenebis(salicylideneimine)