C₂₆⁽¹³⁾C₂H₂₅BrO₆

Base Information

• Chemical Name: C₂₆⁽¹³⁾C₂H₂₅BrO₆
• CAS No.: 760988-01-0
• Molecular Formula: C₂₈H₂₅BrO₆
• Molecular Weight: 539.385
• Mol file: 760988-01-0.mol

Synonyms:C₂₆⁽¹³⁾C₂H₂₅BrO₆

Chemical Property of C₂₆⁽¹³⁾C₂H₂₅BrO₆

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₆⁽¹³⁾C₂H₂₅BrO₆

There total 1 articles about C₂₆⁽¹³⁾C₂H₂₅BrO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

methyl 5-formyl-2-methoxybenzoate (78515-16-9) + C14(13)C2H27BrO6P2 (760988-00-9) → C26(13)C2H25BrO6 (760988-01-0)

Guidance literature:

With sodium methylate; In methanol; Heating;

DOI:10.1016/j.ejmech.2004.02.013

Reference yield:

C26(13)C2H25BrO6 (760988-01-0) → C24(13)C2H21BrO6

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃;

DOI:10.1016/j.ejmech.2004.02.013

Reference yield:

C26(13)C2H25BrO6 (760988-01-0) → C22(13)C2H17BrO6

Guidance literature:

Multi-step reaction with 2 steps

1: BBr₃ / CH₂Cl₂ / -78 - 20 °C

2: 50 percent / KOH / H₂O / 4 h / Heating

With potassium hydroxide; boron tribromide; In dichloromethane; water;

DOI:10.1016/j.ejmech.2004.02.013

upstream raw materials:

methyl 5-formyl-2-methoxybenzoate

C₁₄⁽¹³⁾C₂H₂₇BrO₆P₂