octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside

Base Information

Chemical Name:octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside
CAS No.:1194234-22-4
Molecular Formula:C₃₁H₄₃NO₉
Molecular Weight:573.684
Hs Code.:

Synonyms:octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside

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Chemical Property of octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside

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Technology Process of octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside

There total 8 articles about octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 14470-30-5
N^α-benzyloxycarbonyl-L-phenylalanine anhydride

: 29836-26-8
n-octyl β-D-glucopyranoside

: 1194234-22-4
octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside

Guidance literature:: n-octyl β-D-glucopyranoside; With 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(1H-indol-3-yl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine; In chloroform; at -20 - 20 ℃;

N^α-benzyloxycarbonyl-L-phenylalanine anhydride; In chloroform; at -20 ℃; for 24h; regioselective reaction;
DOI:10.1021/jo901569v

Reference yield: 82.0%

: 1161-13-3
N-Cbz-L-Phe

: 29836-26-8
n-octyl β-D-glucopyranoside

: 1194234-22-4
octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside

Guidance literature:: N-Cbz-L-Phe; With pivaloyl chloride; N-ethyl-N,N-diisopropylamine; In chloroform; at 20 ℃; for 1h; Inert atmosphere;

n-octyl β-D-glucopyranoside; With 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(1H-indol-3-yl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine; In chloroform; at -20 ℃; for 24h; Reagent/catalyst; regioselective reaction; Catalytic behavior; Inert atmosphere;
DOI:10.1021/jo301007x

Reference yield: 50.0%

: 1194234-37-1
C₄₀H₆₁NO₉Si

: 1194234-38-2
C₄₀H₆₁NO₉Si

: C₃₁H₄₃NO₉

: 1194234-22-4
octyl 4-O-((S)-2-benzyloxycarbonylamino-3-phenylpropanoyl)-β-D-glucopyranoside

Guidance literature:: C₄₀H₆₁NO₉Si; C₄₀H₆₁NO₉Si; With pyridinium p-toluenesulfonate; In ethanol; at 0 - 20 ℃;

With water; In ethanol;
DOI:10.1021/jo901569v