2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid

Base Information

Chemical Name:2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid
CAS No.:1192314-96-7
Molecular Formula:C₃₁H₂₈N₂O₈S
Molecular Weight:588.638
Hs Code.:

Synonyms:2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid

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Chemical Property of 2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid

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Technology Process of 2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid

There total 6 articles about 2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1192314-95-6
2-(4-butylbenzamido)-5-(3-(methoxycarbonyl)-4-(phenylsulfonamido)phenoxy)-benzoic acid

: 1192314-96-7
2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid

Guidance literature:: 2-(4-butylbenzamido)-5-(3-(methoxycarbonyl)-4-(phenylsulfonamido)phenoxy)-benzoic acid; With water; sodium hydroxide; In ethanol; at 85 ℃; for 0.5h;

With hydrogenchloride; In ethanol; water; pH=3;

Reference yield:

: 1192318-99-2
methyl 5-hydroxy-2-[(phenylsulfonyl)amino]benzoate

: 1192314-96-7
2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / DMF (N,N-dimethylformamide) / 24 h / 120 °C

1.2: pH 5

2.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h / 2280.15 Torr

3.1: triethylamine / tetrahydrofuran / 20 °C

4.1: water; sodium hydroxide / ethanol / 0.5 h / 85 °C

4.2: pH 3

With water; hydrogen; potassium carbonate; triethylamine; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethylformamide); ethanol;

Reference yield:

: 1192319-00-8
5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid

: 1192314-96-7
2-(4-butylbenzamido)-5-(3-carboxy)-4-(phenylsulfonamido)phenoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 16 h / 2280.15 Torr

2.1: triethylamine / tetrahydrofuran / 20 °C

3.1: water; sodium hydroxide / ethanol / 0.5 h / 85 °C

3.2: pH 3

With water; hydrogen; triethylamine; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol;