5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid

Base Information

Chemical Name:5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid
CAS No.:1192319-00-8
Molecular Formula:C₂₁H₁₆N₂O₉S
Molecular Weight:472.432
Hs Code.:

Synonyms:5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid

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Chemical Property of 5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid

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Technology Process of 5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid

There total 2 articles about 5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 320-98-9
5-fluoro-2-nitrobenzoic acid

: 1192318-99-2
methyl 5-hydroxy-2-[(phenylsulfonyl)amino]benzoate

: 1192319-00-8
5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid

Guidance literature:: 5-fluoro-2-nitrobenzoic acid; methyl 5-hydroxy-2-[(phenylsulfonyl)amino]benzoate; With potassium carbonate; In DMF (N,N-dimethylformamide); at 120 ℃; for 24h;

With hydrogenchloride; In DMF (N,N-dimethylformamide); water; pH=5;

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 1192319-00-8
5-(3-(methoxycarbonyl)-4-[(phenylsulfonyl)amino]phenoxy)-2-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 48 h / Reflux

1.3: pH 8

2.1: pyridine / 0 - 20 °C

3.1: potassium carbonate / DMF (N,N-dimethylformamide) / 24 h / 120 °C

3.2: pH 5

With pyridine; sulfuric acid; potassium carbonate; In DMF (N,N-dimethylformamide);