N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea

Base Information

• Chemical Name: N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea
• CAS No.: 143224-64-0
• Molecular Formula: C₁₉H₃₃N₃O₂
• Molecular Weight: 335.49

Synonyms:N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea

Chemical Property of N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea

Chemical Property:

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Technology Process of N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea

There total 6 articles about N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.4%

N-[3S-[N-(phenylmethyl)amino]-2R-hydroxy-4-phenylbutyl]-N'-(1,1-dimethylethyl)-N-(2-methylpropyl)urea (170359-27-0) → N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea (143224-64-0)

Guidance literature:

palladium; In ethanol;

Reference yield: 93.4%

→ N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea (143224-64-0)

Guidance literature:

Reference yield:

N-<3S--2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethyl-ethyl)-N-(2-methylpropyl)urea (171370-12-0) → N-<(3S-amino)-2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethylethyl)-N-(2-methyl-propyl)urea (143224-64-0)

Guidance literature:

With hydrogen; palladium dihydroxide; In ethanol; for 8h; under 3102.9 Torr; Yield given;

DOI:10.1016/0040-4020(95)00309-V

upstream raw materials:

N-<3S--2R-hydroxy-4-phenylbutyl>-N'-(1,1-dimethyl-ethyl)-N-(2-methylpropyl)urea

N-benzyloxycarbonyl-3(S)-amino-1,2(S)epoxy-4-phenylbutane

(S)-benzyl (4-chloro-3-oxo-1-phenylbutan-2-yl)carbamate

N-benzyloxycarbonyl-3(S)-amino-1-chloro-4-phenyl-2(S)-butanol

Downstream raw materials:

{(S)-1-[(1S,2R)-1-Benzyl-3-(3-tert-butyl-1-isobutyl-ureido)-2-hydroxy-propylcarbamoyl]-2-carbamoyl-ethyl}-carbamic acid benzyl ester

Telinavir

(S)-2-Amino-N¹-[(1S,2R)-1-benzyl-3-(3-tert-butyl-1-isobutyl-ureido)-2-hydroxy-propyl]-succinamide

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