Technology Process of C43H54O8
There total 12 articles about C43H54O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere
2: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere
With
boron trifluoride diethyl etherate; magnesium dibromide etherate; triethylamine;
In
dichloromethane;
DOI:10.1016/j.steroids.2012.10.021
- Guidance literature:
-
Multi-step reaction with 8 steps
1: pyridine / 6 h / Inert atmosphere
2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 19 h / 0 - 25 °C / Inert atmosphere
3: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
4: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere
5: hydroquinidein 1,4-phthalazinediyl diether; potassium carbonate; potassium hexacyanoferrate(III); potassium osmate(VI) / water; tert-butyl alcohol / 18 h / 0 °C / Inert atmosphere
6: 1H-imidazole; dmap / dichloromethane / 1 h / 25 °C / Inert atmosphere
7: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere
8: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere
With
pyridine; 1H-imidazole; triethylsilane; dmap; potassium osmate(VI); boron trifluoride diethyl etherate; iodine; potassium carbonate; magnesium dibromide etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; triphenylphosphine; potassium hexacyanoferrate(III);
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.steroids.2012.10.021