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C43H54O8

Base Information
  • Chemical Name:C43H54O8
  • CAS No.:1421916-96-2
  • Molecular Formula:C43H54O8
  • Molecular Weight:698.897
  • Hs Code.:
C<sub>43</sub>H<sub>54</sub>O<sub>8</sub>

Synonyms:C43H54O8

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Chemical Property of C43H54O8
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Technology Process of C43H54O8

There total 12 articles about C43H54O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

Guidance literature:
With boron trifluoride diethyl etherate; In dichloromethane; for 1h; Inert atmosphere;
DOI:10.1016/j.steroids.2012.10.021
Guidance literature:
Multi-step reaction with 2 steps
1: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere
2: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere
With boron trifluoride diethyl etherate; magnesium dibromide etherate; triethylamine; In dichloromethane;
DOI:10.1016/j.steroids.2012.10.021
Guidance literature:
Multi-step reaction with 8 steps
1: pyridine / 6 h / Inert atmosphere
2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 19 h / 0 - 25 °C / Inert atmosphere
3: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
4: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere
5: hydroquinidein 1,4-phthalazinediyl diether; potassium carbonate; potassium hexacyanoferrate(III); potassium osmate(VI) / water; tert-butyl alcohol / 18 h / 0 °C / Inert atmosphere
6: 1H-imidazole; dmap / dichloromethane / 1 h / 25 °C / Inert atmosphere
7: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere
8: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere
With pyridine; 1H-imidazole; triethylsilane; dmap; potassium osmate(VI); boron trifluoride diethyl etherate; iodine; potassium carbonate; magnesium dibromide etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; triphenylphosphine; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.steroids.2012.10.021
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