3-(3-methylphenoxy)-5-nitroaniline

Base Information

• Chemical Name: 3-(3-methylphenoxy)-5-nitroaniline
• CAS No.: 352637-09-3
• Molecular Formula: C₁₃H₁₂N₂O₃
• Molecular Weight: 244.25
• Mol file: 352637-09-3.mol

Synonyms:3-nitro-5-(m-tolyloxy)phenylamine

Chemical Property of 3-(3-methylphenoxy)-5-nitroaniline

Chemical Property:

Purity/Quality:

3-Nitro-5-(m-tolyloxy)aniline 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(3-methylphenoxy)-5-nitroaniline

There total 4 articles about 3-(3-methylphenoxy)-5-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-Dinitro-5-m-tolyloxy-benzene → 3-nitro-5-(m-tolyloxy)phenylamine (352637-09-3)

Guidance literature:

With diammonium sulfide; In ethanol; at 75 ℃; for 1h;

DOI:10.1016/j.bmcl.2014.09.039

Reference yield:

3-methyl-phenol (108-39-4) → 3-nitro-5-(m-tolyloxy)phenylamine (352637-09-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 80 °C

2: diammonium sulfide / ethanol / 1 h / 75 °C

With diammonium sulfide; potassium carbonate; In 1-methyl-pyrrolidin-2-one; ethanol;

DOI:10.1016/j.bmcl.2014.09.039

Reference yield:

1,3,5-trinitrobenzene (99-35-4) → 3-nitro-5-(m-tolyloxy)phenylamine (352637-09-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 80 °C

2: diammonium sulfide / ethanol / 1 h / 75 °C

With diammonium sulfide; potassium carbonate; In 1-methyl-pyrrolidin-2-one; ethanol;

DOI:10.1016/j.bmcl.2014.09.039

upstream raw materials:

3-methyl-phenol

1,3,5-trinitrobenzene