benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside

Base Information

Chemical Name:benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside
CAS No.:104875-52-7
Molecular Formula:C₂₁H₂₀F₃N₃O₇S
Molecular Weight:515.467
Hs Code.:

Synonyms:benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside

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Technology Process of benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside

There total 1 articles about benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26531-94-2
benzyl 2,3-anhydro-4,6-O-benzylidene-β-D-talopyranoside

: 104875-52-7
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / sodium azide, ammonium chloride / 2-methoxy-ethanol; H₂O / 140 °C

2: 90 percent / pyridine / 5 h / Ambient temperature

With pyridine; sodium azide; ammonium chloride; In 2-methoxy-ethanol; water;
DOI:10.1021/jo00374a013