Technology Process of C18H32O3Si
There total 8 articles about C18H32O3Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ammonium chloride; zinc / tetrahydrofuran; water / 0 - 25 °C
2: macroporous acrylic resin-immobilized Candida antarctica lipase B / di-isopropyl ether / 70 h / 25 °C / Inert atmosphere; Enzymatic reaction
3: 1H-imidazole; dmap / dichloromethane / 18 h / 25 °C / Inert atmosphere
4: 4-methylmorpholine N-oxide / water; tert-butyl alcohol / 12 h / Reflux
With
1H-imidazole; dmap; ammonium chloride; 4-methylmorpholine N-oxide; zinc;
In
tetrahydrofuran; dichloromethane; di-isopropyl ether; water; tert-butyl alcohol;
1: |Barbier Coupling Reaction;
DOI:10.1016/j.tetasy.2012.06.015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: macroporous acrylic resin-immobilized Candida antarctica lipase B / di-isopropyl ether / 70 h / 25 °C / Inert atmosphere; Enzymatic reaction
2: 1H-imidazole; dmap / dichloromethane / 18 h / 25 °C / Inert atmosphere
3: 4-methylmorpholine N-oxide / water; tert-butyl alcohol / 12 h / Reflux
With
1H-imidazole; dmap; 4-methylmorpholine N-oxide;
In
dichloromethane; di-isopropyl ether; water; tert-butyl alcohol;
DOI:10.1016/j.tetasy.2012.06.015