3-<methyl>-6-phenoxy-1,4-dimethylcarbazole

Base Information

Chemical Name:3-<methyl>-6-phenoxy-1,4-dimethylcarbazole
CAS No.:157060-86-1
Molecular Formula:C₃₄H₃₈N₂O₅S
Molecular Weight:586.752
Hs Code.:

3-<<N-tosyl(2,2-diethoxyethyl)amino>methyl>-6-phenoxy-1,4-dimethylcarbazole

Synonyms:3-<methyl>-6-phenoxy-1,4-dimethylcarbazole

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Chemical Property of 3-<methyl>-6-phenoxy-1,4-dimethylcarbazole

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Technology Process of 3-<methyl>-6-phenoxy-1,4-dimethylcarbazole

There total 5 articles about 3-<methyl>-6-phenoxy-1,4-dimethylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 98-59-9
p-toluenesulfonyl chloride

: 157060-85-0
3-<<(2,2-diethoxyethyl)amino>methyl>-1,4-dimethyl-6-phenoxycarbazole

: 157060-86-1
3-<methyl>-6-phenoxy-1,4-dimethylcarbazole

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; at 22 ℃; for 2h;
DOI:10.1021/jm00039a007

Reference yield:

: 645-36-3
2,2-diethoxy-ethanamine

: 157060-86-1
3-<methyl>-6-phenoxy-1,4-dimethylcarbazole

Guidance literature:: Multi-step reaction with 3 steps

1: 3 h / 110 - 115 °C

2: 90 percent / NaBH₄ / methanol / 1 h / 22 °C

3: 89 percent / Na₂CO₃ / tetrahydrofuran; H₂O / 2 h / 22 °C

With sodium tetrahydroborate; sodium carbonate; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm00039a007

Reference yield:

: 157060-91-8
1,4-dimethyl-6-phenoxycarbazole

: 157060-86-1
3-<methyl>-6-phenoxy-1,4-dimethylcarbazole

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / POCl₃ / 1,2-dichloro-benzene / 4 h / 105 °C

2: 3 h / 110 - 115 °C

3: 90 percent / NaBH₄ / methanol / 1 h / 22 °C

4: 89 percent / Na₂CO₃ / tetrahydrofuran; H₂O / 2 h / 22 °C

With sodium tetrahydroborate; sodium carbonate; trichlorophosphate; In tetrahydrofuran; methanol; water; 1,2-dichloro-benzene;
DOI:10.1021/jm00039a007