(S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate

Base Information

Chemical Name:(S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate
CAS No.:1276113-62-2
Molecular Formula:C₁₇H₂₂F₃NO₇S
Molecular Weight:441.425
Hs Code.:

Synonyms:(S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate

There total 3 articles about (S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1276113-56-4
methyl (3 S)-3-(tert-butoxycarbonylamino)-4-hydroxy-4-(2,4,5-trifluorophenyl)butyrate

: 124-63-0
methanesulfonyl chloride

: 1276113-62-2
(S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate

Guidance literature:: In dichloromethane; at -20 - 20 ℃;

Reference yield:

: 909295-29-0
methyl (S)-3-((tert-butoxycarbonyl)amino)-4-oxobutanoate

: 1276113-62-2
(S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; magnesium / tetrahydrofuran / 3 h / 30 - 40 °C

1.2: -20 - 20 °C

2.1: dichloromethane / -20 - 20 °C

With iodine; magnesium; In tetrahydrofuran; dichloromethane;

Reference yield:

: 327-52-6
1-bromo-2,4,5-trifluorobenzene

: 1276113-62-2
(S)-methyl 3-(tert-butoxycarbonylamino)-4-(trifluoromethanesulfonate)-4-(2,4,5-trifluorophenyl)-n-butyrate

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine; magnesium / tetrahydrofuran / 3 h / 30 - 40 °C

1.2: -20 - 20 °C

2.1: dichloromethane / -20 - 20 °C

With iodine; magnesium; In tetrahydrofuran; dichloromethane;