(2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

Base Information

Chemical Name:(2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane
CAS No.:1186132-07-9
Molecular Formula:C₄₈H₆₃N₃O₅Si
Molecular Weight:790.131
Hs Code.:

Synonyms:(2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

Suppliers and Price of (2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

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Technology Process of (2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

There total 3 articles about (2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 916159-68-7
(2S,3S,4R)-2-azido-1-(tert-butyldiphenylsilyloxy)octadecane-3,4-diol

: 98-88-4
benzoyl chloride

: 1186132-07-9
(2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

Guidance literature:: With pyridine;
DOI:10.1016/j.bmcl.2009.05.095

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1186132-07-9
(2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; pyridine / dichloromethane / 48 h / Inert atmosphere

2: dmap; pyridine / Inert atmosphere

With pyridine; dmap; In dichloromethane;

Reference yield:

: 117168-59-9
(2S,3S,4R)-2-azido-1,3,4-octadecanetriol

: 1186132-07-9
(2S,3S,4R)-2-azido-(3,4-dibenzoyloxy-1-tert-butyldiphenylsilyloxy)octadecane

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; pyridine / dichloromethane / 48 h / Inert atmosphere

2: dmap; pyridine / Inert atmosphere

With pyridine; dmap; In dichloromethane;