C₂₈H₃₃BrFN₃O₃Si

Base Information

Chemical Name:C₂₈H₃₃BrFN₃O₃Si
CAS No.:1420206-07-0
Molecular Formula:C₂₈H₃₃BrFN₃O₃Si
Molecular Weight:586.576
Hs Code.:

C<sub>28</sub>H<sub>33</sub>BrFN<sub>3</sub>O<sub>3</sub>Si

Synonyms:C₂₈H₃₃BrFN₃O₃Si

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Chemical Property of C₂₈H₃₃BrFN₃O₃Si

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Technology Process of C₂₈H₃₃BrFN₃O₃Si

There total 6 articles about C₂₈H₃₃BrFN₃O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1420205-53-3
C₁₁H₁₃FN₂O

: 1420205-90-8
C₁₇H₂₃Br₂NO₃Si

: 1420206-07-0
C₂₈H₃₃BrFN₃O₃Si

Guidance literature:: With sodium carbonate; at 20 ℃;

Reference yield:

: 1420205-85-1
ethyl 5-bromo-4-methoxy-1-(2-trimethylsilylethoxymethyl)indole-2-carboxylate

: 1420206-07-0
C₂₈H₃₃BrFN₃O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; lithium hydroxide / ethanol / 1 h / 20 °C

2.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3.1: hexane; acetonitrile / -5 - 20 °C

3.2: 0.33 h / Cooling with ice

4.1: sodium carbonate / 20 °C

With oxalyl dichloride; water; sodium carbonate; lithium hydroxide; In ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1420205-82-8
ethyl (Z)-2-azido-3-(3-bromo-2-methoxy-phenyl)prop-2-enoate

: 1420206-07-0
C₂₈H₃₃BrFN₃O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 5,5-dimethyl-1,3-cyclohexadiene / 1 h / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

2.2: 0 - 20 °C

3.1: water; lithium hydroxide / ethanol / 1 h / 20 °C

4.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

5.1: hexane; acetonitrile / -5 - 20 °C

5.2: 0.33 h / Cooling with ice

6.1: sodium carbonate / 20 °C

With oxalyl dichloride; water; sodium hydride; sodium carbonate; lithium hydroxide; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;