thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester

Base Information

• Chemical Name: thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester
• CAS No.: 910111-75-0
• Molecular Formula: C₁₆H₂₂FNO₃S
• Molecular Weight: 327.42

Synonyms:thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester

Chemical Property of thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester

Chemical Property:

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Technology Process of thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester

There total 1 articles about thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanesulphonic acid 2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl ester (910111-74-9) + potassium thioacetate (10387-40-3) → thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester (910111-75-0)

Guidance literature:

In N,N-dimethyl-formamide; for 20h;

Reference yield:

thioacetic acid S-[2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl] ester (910111-75-0) + tetra(n-butyl)ammonium hydroxide (2052-49-5) → (R)-2-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propane-1-sulphonate tetra-n-butyl ammonium salt (910111-77-2)

Guidance literature:

With Oxone; In methanol; water; at 20 ℃; for 12.5h;

upstream raw materials:

methanesulphonic acid 2(R)-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propyl ester

potassium thioacetate

Downstream raw materials:

(R)-2-tert-butoxycarbonylamino-3-(2-fluoro-phenyl)-propane-1-sulphonate tetra-n-butyl ammonium salt

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