Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

Base Information

• Chemical Name: Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃
• CAS No.: 98736-79-9
• Molecular Formula: CF₃O₃S*C₂₈H₂₂CrN₂O₃
• Molecular Weight: 635.561

Synonyms:Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

Chemical Property of Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

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Technology Process of Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

There total 3 articles about Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-ethylenebis(α-phenylsalicylideneiminate) (65940-45-6) → Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O)(1+)*CF3SO2O(1-)=(Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O))OSO2CF3 (98736-79-9)

Guidance literature:

Multi-step reaction with 2 steps

1: air / acetone

2: acetonitrile

With air; In acetone; acetonitrile;

DOI:10.1021/ja00311a064

Reference yield:

Cr(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O)(1+)*CF3SO2O(1-)=(Cr(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O))OSO2CF3 (98736-62-0) + iodosylbenzene (536-80-1) → Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O)(1+)*CF3SO2O(1-)=(Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O))OSO2CF3 (98736-79-9)

Guidance literature:

In acetonitrile; a suspn. of Cr-complex and PhIO in MeCN was stirred for 30 min; soln. was filtered, anhyd. ether added to the filtrate, resulting ppt. was collected by filtration;

DOI:10.1021/ja00311a064

Reference yield:

[7,7'-diphenyl-N,N'-ethylenebis(salicylideneaminato)]chromium(III)triflate dihydrate (99356-22-6) + iodosylbenzene (536-80-1) → Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O)(1+)*CF3SO2O(1-)=(Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O))OSO2CF3 (98736-79-9)

Guidance literature:

In acetonitrile; byproducts: C6H5I, H2O; addn. of iodosylbenzene (slight excess) to Cr complex soln.; stirring slurry, 30 min; filtration; slow addn. of anhydrous ether; pptn.;

upstream raw materials:

[7,7'-diphenyl-N,N'-ethylenebis(salicylideneaminato)]chromium(III)triflate dihydrate

iodosylbenzene

Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

N,N'-ethylenebis(α-phenylsalicylideneiminate)

Downstream raw materials:

[7,7'-diphenyl-N,N'-ethylenebis(salicylideneaminato)]oxochromium(V), chloride adduct

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