1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

Base Information

Chemical Name:1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole
CAS No.:366498-82-0
Molecular Formula:C₂₃H₁₉BrFeN₂O₄
Molecular Weight:523.166
Hs Code.:

Synonyms:1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

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Chemical Property of 1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

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Technology Process of 1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

There total 3 articles about 1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (3R*p,4R*,5S*)-1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenyl-4,5-dihydropyrazole

: 366498-82-0
1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; the Fe complex and the quinone were dissolved in CH2Cl2, stirred at roomtemp. for 6 h; evapd. to dryness, residue recrystd. from ethanol; elem. anal.;
DOI:10.1016/S0022-2860(01)00429-X

Reference yield: 76.0%

: (3R*p,4R*,5S*)-1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenyl-4,5-dihydropyrazole

: 624-49-7
dimethylfumarate

: 366498-82-0
1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

Guidance literature:: In acetonitrile; mixt. was stirred and refluxed in the presence of molecular sieves underAr for 6 h; solvent was evapd. to dryness, residue was chromd. and recrystd. from EtOH; elem. anal.;
DOI:10.1016/S0022-2860(01)00429-X

Reference yield: 69.0%

: 366498-71-7
N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine

: 624-49-7
dimethylfumarate

: 366498-82-0
1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

Guidance literature:: In acetonitrile; mixt. was stirred and refluxed in the presence of molecular sieves underAr for 6 h; solvent was evapd. to dryness, residue was chromd. and recrystd. from EtOH; elem. anal.;
DOI:10.1016/S0022-2860(01)00429-X