N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine

Base Information

Chemical Name:N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine
CAS No.:366498-71-7
Molecular Formula:C₁₇H₁₅BrFeN₂
Molecular Weight:383.07
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine

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Technology Process of N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine

There total 1 articles about N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 12093-10-6
ferrocenecarboxaldehyde

: 589-21-9
(4-bromophenyl)hydrazine

: 366498-71-7
N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine

Guidance literature:: formyl ferrocene and the pyridazinone were condensed according proceduredescribed by A. Abran, A. Csampai, V. Harmath, P. Sohar, Models in Chem istry, Acta Chim. Hung. 135 (1998) 439-447.; elem. anal.;
DOI:10.1016/S0022-2860(01)00429-X

Reference yield: 82.0%

: 366498-71-7
N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine

: 624-49-7
dimethylfumarate

: (3R*p,4R*,5S*)-1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenyl-4,5-dihydropyrazole

Guidance literature:: In acetonitrile; mixt. was stirred and heated at 70°C in the presence of molecularsieves under Ar for 3 h; solvent was evapd. to dryness, residue was chromd. and recrystd. from EtOH; elem. anal.;
DOI:10.1016/S0022-2860(01)00429-X

Reference yield: 69.0%

: 366498-71-7
N-(4-bromophenyl)-N'-ferrocenylmethylidenehydrazine

: 624-49-7
dimethylfumarate

: 366498-82-0
1-(4-bromophenyl)-4,5-bis-carbomethoxy-3-ferrocenylpyrazole

Guidance literature:: In acetonitrile; mixt. was stirred and refluxed in the presence of molecular sieves underAr for 6 h; solvent was evapd. to dryness, residue was chromd. and recrystd. from EtOH; elem. anal.;
DOI:10.1016/S0022-2860(01)00429-X