1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

Base Information

Chemical Name:1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane
CAS No.:651301-61-0
Molecular Formula:C₄₁H₅₃O₁₀P₃
Molecular Weight:798.787
Hs Code.:

Synonyms:1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

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Chemical Property of 1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

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Technology Process of 1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

There total 1 articles about 1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 122-52-1
triethyl phosphite

: 651302-01-1
1,1,1-tris[4-(bromomethyl)phenyl]-1-[4-(1,1-dimethoxymethyl)phenyl]methane

: 651301-61-0
1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

Guidance literature:: at 100 ℃; for 6h;

Reference yield: 77.0%

: 109-97-7,30604-81-0
pyrrole

: 651301-61-0
1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

: 651301-66-5
5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

Guidance literature:: With indium(III) chloride; at 20 ℃; for 1.5h;
DOI:10.1021/jo034946d

Reference yield:

: 651301-61-0
1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

: 5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]-10,15,20-tri-p-tolylporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1.1: 77 percent / InCl₃ / 1.5 h / 20 °C

2.1: InCl₃ / CH₂Cl₂ / 1 h / 20 °C

2.2: DDQ / CH₂Cl₂ / 1 h

With indium(III) chloride; In dichloromethane;
DOI:10.1021/jo034946d