5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

Base Information

Chemical Name:5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane
CAS No.:651301-66-5
Molecular Formula:C₄₉H₆₁N₂O₉P₃
Molecular Weight:914.953
Hs Code.:

Synonyms:5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

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Chemical Property of 5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

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Technology Process of 5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

There total 2 articles about 5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 109-97-7,30604-81-0
pyrrole

: 651301-61-0
1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]-1-(4-formylphenyl)methane

: 651301-66-5
5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

Guidance literature:: With indium(III) chloride; at 20 ℃; for 1.5h;
DOI:10.1021/jo034946d

Reference yield:

: 651302-01-1
1,1,1-tris[4-(bromomethyl)phenyl]-1-[4-(1,1-dimethoxymethyl)phenyl]methane

: 651301-66-5
5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

Guidance literature:: Multi-step reaction with 2 steps

1: 2.89 g / 6 h / 100 °C

2: 77 percent / InCl₃ / 1.5 h / 20 °C

With indium(III) chloride;
DOI:10.1021/jo034946d

Reference yield:

: 266341-19-9
1,9-bis(benzoyl)-5-(4-methylphenyl)dipyrromethane-diol

: 651301-66-5
5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane

: C₈₁H₈₃N₄O₉P₃

Guidance literature:: 1,9-bis(benzoyl)-5-(4-methylphenyl)dipyrromethane-diol; 5-[4-[1,1,1-tris[4-(diethoxyphosphorylmethyl)phenyl]methyl]phenyl]dipyrromethane; indium(III) chloride; In dichloromethane; at 20 ℃; for 1h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 1h;

With triethylamine; In dichloromethane;