C₈H₄INO

Base Information

• Chemical Name: C₈H₄INO
• CAS No.: 1086429-91-5
• Molecular Formula: C₈H₄INO
• Molecular Weight: 257.03
• Mol file: 1086429-91-5.mol

Synonyms:C₈H₄INO

Chemical Property of C₈H₄INO

Chemical Property:

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Technology Process of C₈H₄INO

There total 1 articles about C₈H₄INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-iodo-3-methylbenzonitrile (52107-70-7) → 2-bromo-3-cyanobenzaldehyde (446864-55-7) + C8H4INO (1086429-91-5)

Guidance literature:

2-iodo-3-methylbenzonitrile; With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 85 ℃; for 22h; Inert atmosphere;

With sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 - 100 ℃; Inert atmosphere;

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 65 ℃; for 0.666667h; Inert atmosphere;

DOI:10.1021/ol801986m

upstream raw materials:

2-iodo-3-methylbenzonitrile

Refernces