Nogarene

Base Information

Chemical Name:Nogarene
CAS No.:71582-54-2
Molecular Formula:C27H27NO8
Molecular Weight:493.5052
Hs Code.:
NSC Number:269149
DSSTox Substance ID:DTXSID20395920
ChEMBL ID:CHEMBL1993089

Synonyms:Nogarene;71582-54-2;NCI60_002189;CHEMBL1993089;NOGARENE, U-52048;DTXSID20395920;NSC269149;NSC-269149

Suppliers and Price of Nogarene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Nogarene

Chemical Property:

Vapor Pressure:1.59E-32mmHg at 25°C
Boiling Point:872.4°C at 760 mmHg
Flash Point:481.4°C
Density:1.56g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:1
Exact Mass:491.15801676
Heavy Atom Count:36
Complexity:927

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=CC3=C(C(=C2C=C1)O)C(=O)C4=C(C=C5C(=C4C3=O)OC6C(C(C(C5(O6)C)O)N(C)C)O)O

Technology Process of Nogarene

There total 21 articles about Nogarene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: (+)-2',4'-di-O-acetylnogarene

: 71582-54-2
(+)-nogarene

Guidance literature:: With hydrogenchloride; for 12h; Heating;
DOI:10.1016/S0040-4039(00)84471-8

Reference yield: 87.0%

: 105827-65-4
(+)-2',4'-di-O-acetylnogarene

: 71582-54-2
(+)-nogarene

Guidance literature:: With hydrogenchloride; for 15h; Heating;
DOI:10.1016/S0040-4020(01)81433-2

Reference yield:

: 105827-63-2
2,6-dimethyl-1,3-cyclohexadiene-1-carboxylic acid

: 71582-54-2
(+)-nogarene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) LDA / 1.) THF, -60 deg C, 2.) THF, r.t.

2: 85 percent / tetrahydrofuran / 0.5 h / Ambient temperature

3: 85 percent / DDQ, CSA / benzene / 5 h / Heating

4: 87 percent / 1N HCl / 12 h / Heating

With hydrogenchloride; camphor-10-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4039(00)84471-8