ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate

Base Information

Chemical Name:ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate
CAS No.:1224727-68-7
Molecular Formula:C₁₄H₁₇NO₆
Molecular Weight:295.292
Hs Code.:

Synonyms:ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate

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Chemical Property of ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate

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Technology Process of ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate

There total 3 articles about ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2969-81-5
Ethyl 4-bromobutyrate

: 30879-49-3
1-(5-hydroxy-2-nitrophenyl)ethan-1-one

: 1224727-68-7
ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 121h; Inert atmosphere;
DOI:10.1021/ja305280w

Reference yield:

: 1392043-83-2
bis(3-acetylphenyl) oxalate

: 1224727-68-7
ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; nitric acid / 0.5 h / -20 - -10 °C / Inert atmosphere

1.2: 0.5 h / -10 - 5 °C / Inert atmosphere

1.3: 48 h / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 121 h / Inert atmosphere

With sulfuric acid; nitric acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ja305280w

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 1224727-68-7
ethyl 4-(3-acetyl-4-nitrophenoxy)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / ethyl acetate / 12 h / 0 - 20 °C / Inert atmosphere

2.1: sulfuric acid; nitric acid / 0.5 h / -20 - -10 °C / Inert atmosphere

2.2: 0.5 h / -10 - 5 °C / Inert atmosphere

2.3: 48 h / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 121 h / Inert atmosphere

With sulfuric acid; nitric acid; potassium carbonate; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja305280w