2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

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Chemical Name:2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine
CAS No.:1286246-51-2
Molecular Formula:C₁₇H₂₅N₃O
Molecular Weight:287.405
Hs Code.:

Synonyms:2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

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Chemical Property of 2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

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Technology Process of 2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

There total 2 articles about 2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1285259-24-6
1,3,4-trimethyl-1H-pyrazol-5-yl trifluoromethanesulfonate

: 1286246-78-3
2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

: 1286246-51-2
2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 85 ℃; Inert atmosphere;

Reference yield:

: 166386-49-8
2-(5-bromo-2-methoxyphenyl)-N,N-dimethylethanamine

: 1286246-51-2
2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 3 h / -78 °C / Inert atmosphere

1.3: 20 °C

2.1: potassium carbonate / 1,2-dimethoxyethane; water / Inert atmosphere

2.2: 5 h / 85 °C / Inert atmosphere

With n-butyllithium; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; hexane; water;

Reference yield: 35.0%

: 1286246-51-2
2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

: 1286246-52-3
2-(2-(dimethylamino)ethyl)-4-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenol

Guidance literature:: 2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine; With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;

With methanol; In dichloromethane;