2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

Base Information

Chemical Name:2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine
CAS No.:1286246-78-3
Molecular Formula:C₁₇H₂₈BNO₃
Molecular Weight:305.225
Hs Code.:

Synonyms:2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

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Chemical Property of 2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

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Technology Process of 2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

There total 1 articles about 2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 166386-49-8
2-(5-bromo-2-methoxyphenyl)-N,N-dimethylethanamine

: 1286246-78-3
2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

Guidance literature:: 2-(5-bromo-2-methoxyphenyl)-N,N-dimethylethanamine; With n-butyllithium; In tetrahydrofuran; hexanes; for 1h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexanes; for 3h; Inert atmosphere;

Reference yield: 43.0%

: 1285259-24-6
1,3,4-trimethyl-1H-pyrazol-5-yl trifluoromethanesulfonate

: 1286246-78-3
2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

: 1286246-51-2
2-(2-methoxy-5-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenyl)-N,N-dimethylethanamine

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 85 ℃; Inert atmosphere;

Reference yield:

: 1285259-24-6
1,3,4-trimethyl-1H-pyrazol-5-yl trifluoromethanesulfonate

: 1286246-78-3
2-(2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-N,N-dimethylethanamine

: 1286246-52-3
2-(2-(dimethylamino)ethyl)-4-(1,3,4-trimethyl-1H-pyrazol-5-yl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 85 °C / Inert atmosphere

2: boron tribromide / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With boron tribromide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; dichloromethane; water;