trans-7-(4-hydroxycyclohexyl)heptanoic acid

Base Information

Chemical Name:trans-7-(4-hydroxycyclohexyl)heptanoic acid
CAS No.:107228-92-2
Molecular Formula:C₁₃H₂₄O₃
Molecular Weight:228.332
Hs Code.:

Synonyms:trans-7-(4-hydroxycyclohexyl)heptanoic acid

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Chemical Property of trans-7-(4-hydroxycyclohexyl)heptanoic acid

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Technology Process of trans-7-(4-hydroxycyclohexyl)heptanoic acid

There total 3 articles about trans-7-(4-hydroxycyclohexyl)heptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 107228-95-5
7-(4-hydroxyphenyl)heptanoic acid

: 107228-92-2
trans-7-(4-hydroxycyclohexyl)heptanoic acid

: 107228-94-4
cis-7-(4-hydroxycyclohexyl)heptanoic acid

Guidance literature:: With hydrogen; Ru-carbon; In ethanol; water; at 102 - 104 ℃; for 1h; under 84583.4 Torr;
DOI:10.1248/cpb.36.178

Reference yield:

: 21244-13-3
7-(4'-methoxyphenyl)heptanoic acid

: 107228-92-2
trans-7-(4-hydroxycyclohexyl)heptanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent HBr / acetic acid

2: 34 percent / hydrogen / 5 percent Ru-C / ethanol; H₂O / 1 h / 102 - 104 °C / 84583.4 Torr

With hydrogen bromide; hydrogen; Ru-carbon; In ethanol; water; acetic acid;
DOI:10.1248/cpb.36.178

Reference yield:

: 21244-11-1
7-(4-methoxy-phenyl)-7-oxo-heptanoic acid

: 107228-92-2
trans-7-(4-hydroxycyclohexyl)heptanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Clemmensen reduction

2: 48 percent HBr / acetic acid

3: 34 percent / hydrogen / 5 percent Ru-C / ethanol; H₂O / 1 h / 102 - 104 °C / 84583.4 Torr

With hydrogen bromide; hydrogen; Ru-carbon; In ethanol; water; acetic acid;
DOI:10.1248/cpb.36.178