(2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol

Base Information

Chemical Name:(2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol
CAS No.:170874-77-8
Molecular Formula:C₂₆H₃₀O₈S
Molecular Weight:502.585
Hs Code.:

(2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-<phenoxy(thiocarbonyl)>hexane-1,2,3,4,5,6-hexol

Synonyms:(2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol

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Technology Process of (2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol

There total 3 articles about (2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 51051-82-2
O³-benzoyl-O¹,O²;O⁵,O⁶-diisopropylidene-D-mannitol

: 1005-56-7
phenylcarbonochloridothioate

: 170874-77-8
(2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol

Guidance literature:: With pyridine; dmap; In dichloromethane; for 24h; Heating;

Reference yield:

: 101864-30-6
O⁴-benzoyl-O¹,O²;O⁵,O⁶-diisopropylidene-D-arabino-[3]hexulose

: 170874-77-8
(2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / Zn(BH₄)2 / diethyl ether / -15 °C

2: 95 percent / pyridine, DMAP / CH₂Cl₂ / 24 h / Heating

With pyridine; dmap; zinc(II) tetrahydroborate; In diethyl ether; dichloromethane;

Reference yield:

: 1707-77-3
1,2:5,6-di-O-isopropylidene-D-mannitol

: 170874-77-8
(2R,3R,4R,5R)-4-O-Benzoyl-1,2;5,6-di-O-isopropylidene-3-O-hexane-1,2,3,4,5,6-hexol

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / pyridine, DMAP / Ambient temperature

2: 95 percent / pyridine, DMAP / CH₂Cl₂ / 24 h / Heating

With pyridine; dmap; In dichloromethane;