4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride

Base Information

Chemical Name:4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride
CAS No.:1333500-34-7
Molecular Formula:C₁₅H₂₃N₅O₃*ClH
Molecular Weight:357.84
Hs Code.:

Synonyms:4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride

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Chemical Property of 4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride

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Technology Process of 4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride

There total 3 articles about 4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.3%

: 1333500-53-0
1-(3,4,5-trimethoxybenzyl)biguanide hydrochloride

: 67-64-1
acetone

: 1333500-34-7
4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride

Guidance literature:: With hydrogenchloride; 2,2-dimethoxy-propane; In methanol; water; Reflux;
DOI:10.1016/j.bmcl.2011.06.125

Reference yield:

: 18638-99-8
3,4,5-trimethoxybenzylamine

: 1333500-34-7
4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / diethyl ether / 20 °C

2: 160 - 180 °C

3: hydrogenchloride; 2,2-dimethoxy-propane / methanol; water / Reflux

With hydrogenchloride; 2,2-dimethoxy-propane; In methanol; diethyl ether; water;
DOI:10.1016/j.bmcl.2011.06.125

Reference yield:

: 42365-69-5
(3,4,5-trimethoxyphenyl)methanamine hydrochloride

: 1333500-34-7
4,6-diamino-1-(3',4',5'-trimethoxybenzyl)-1,2-dihydro-2,2-dimethyl-1,3,5-triazine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 160 - 180 °C

2: hydrogenchloride; 2,2-dimethoxy-propane / methanol; water / Reflux

With hydrogenchloride; 2,2-dimethoxy-propane; In methanol; water;
DOI:10.1016/j.bmcl.2011.06.125