2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine

Base Information

• Chemical Name: 2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine
• CAS No.: 1062320-02-8
• Molecular Formula: C₃₁H₂₆N₆O₂
• Molecular Weight: 514.586

Synonyms:2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine

Chemical Property of 2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine

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Technology Process of 2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine

There total 1 articles about 2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

ortho-anisaldehyde (135-02-4) + 2,4-bis-(phenylamino)-6-(4'-acetylphenylamino)-s-triazine (84688-83-5) → 2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine (1062320-02-8)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield: 69.0%

2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine (1062320-02-8) + malononitrile (109-77-3) → C34H27N9O (1108704-93-3)

Guidance literature:

With ammonium acetate; In ethanol; for 8h; Reflux;

DOI:10.1016/j.ejmech.2009.10.037

Reference yield: 66.0%

2,4-bis-(phenylamino)-6-[4'-{3''-(2'''-methoxyphenyl)-1''-oxo-2''-propen-1''-yl}-phenylamino]-s-triazine (1062320-02-8) + guanidine nitrate (506-93-4) → 2,4-bis-(phenylamino)-6-[4'-{2''-amino-6''-(2'''-methoxyphenyl)-pyrimidin-4''-yl}-phenylamino]-s-triazine (1062320-08-4)

Guidance literature:

With potassium hydroxide; In ethanol; for 10h; Reflux;

DOI:10.1016/j.ejmech.2009.10.037

upstream raw materials:

ortho-anisaldehyde

2,4-bis-(phenylamino)-6-(4'-acetylphenylamino)-s-triazine

Downstream raw materials:

2,4-bis-(phenylamino)-6-[4'-{5''-(2'''-methoxyphenyl)-isoxazol-3''-yl}-phenylamino]-s-triazine

2,4-bis-(phenylamino)-6-[4'-{2''-amino-6''-(2'''-methoxyphenyl)-pyrimidin-4''-yl}-phenylamino]-s-triazine

2,4-bis-(phenylamino)-6-[4'-{2''-(2'''-methoxyphenyl)-2'',3''-dihydro-1'',5''-benzothiazepin-4''-yl}-phenylamino]-s-triazine

C₃₃H₃₀N₈O₂

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