2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid

Base Information

Chemical Name:2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid
CAS No.:1190971-96-0
Molecular Formula:C₁₉H₂₇N₃O₆S
Molecular Weight:425.506
Hs Code.:

Synonyms:2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid

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Chemical Property of 2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid

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Technology Process of 2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid

There total 5 articles about 2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1190972-40-7
C₂₃H₃₅N₃O₆S

: 1190971-96-0
2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid

Guidance literature:: C₂₃H₃₅N₃O₆S; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

With hydrogenchloride; In water;

Reference yield:

: 1190972-38-3
C₁₇H₂₅N₃O₄S

: 1190971-96-0
2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl-ammonium chloride; sodium hydroxide / dichloromethane; water / 0 - 20 °C

2: water; sodium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

With tetrabutyl-ammonium chloride; water; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 874-63-5
3,5-dimethylmethoxybenzene

: 1190971-96-0
2-[2-[N-(1-ethyl-1H-imidazol-2-yl)-methyl-[(4-methoxy-2,6-dimethyl-phenyl)sulfonyl]-amino]-ethoxy]-acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: chlorosulfonic acid / dichloromethane / 0 °C

2.1: triethylamine / dichloromethane / 20 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

4.2: 1 h / Reflux

5.1: tetrabutyl-ammonium chloride; sodium hydroxide / dichloromethane; water / 0 - 20 °C

6.1: water; sodium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

With chlorosulfonic acid; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; tetrabutyl-ammonium chloride; water; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;