3-propanamide

Base Information

• Chemical Name: 3-propanamide
• CAS No.: 133382-98-6
• Molecular Formula: C₁₇H₂₆N₄O₄
• Molecular Weight: 350.418

Synonyms:3-propanamide

Chemical Property of 3-propanamide

Chemical Property:

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Technology Process of 3-propanamide

There total 1 articles about 3-propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

(S)-tert-butyl (1-hydrazinyl-1-oxo-3-phenylpropan-2-yl)carbamate (30189-48-1) + 2-propenamide (79-06-1,12624-24-7,25038-45-3,27754-57-0,33338-03-3,39387-77-4,68247-81-4,9082-06-8,79079-15-5) → 3-propanamide (133382-98-6)

Guidance literature:

In N,N-dimethyl-formamide; at 110 ℃; for 36h;

DOI:10.1016/S0960-894X(99)00049-9

Reference yield: 70.0%

3-propanamide (133382-98-6) + phenyl chloroformate (1885-14-9) → N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester (222853-54-5)

Guidance literature:

With triethylamine; In methanol;

DOI:10.1016/S0960-894X(99)00049-9

Reference yield: 68.0%

3-propanamide (133382-98-6) + benzyl chloroformate (501-53-1,94274-21-2) → N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid benzyl ester (222853-56-7)

Guidance literature:

With triethylamine; In methanol;

DOI:10.1016/S0960-894X(99)00049-9

upstream raw materials:

(S)-tert-butyl (1-hydrazinyl-1-oxo-3-phenylpropan-2-yl)carbamate

2-propenamide

Downstream raw materials:

ethyl (N-tert-butoxycarbonyl-L-phenylalanyl)(2-azaglutaminyl)glycinate

N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid benzyl ester

N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid phenyl ester

N'-(2-tert-butoxycarbonylamino-3-phenyl-propionyl)-N-(2-carbamoyl-ethyl)-hydrazinecarboxylic acid 2,2,2-trichloro-ethyl ester

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