isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Base Information

Chemical Name:isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate
CAS No.:1308254-99-0
Molecular Formula:C₁₈H₂₁BN₂O₆S
Molecular Weight:404.252
Hs Code.:

Synonyms:isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

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Chemical Property of isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

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Technology Process of isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

There total 8 articles about isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1308254-89-8
2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetic acid

: 67-63-0,8013-70-5
isopropyl alcohol

: 1308254-99-0
isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Guidance literature:: sulfuric acid; for 48h; Reflux;

Reference yield:

: 3958-57-4
1-bromomethyl-3-nitrobenzene

: 1308254-99-0
isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Guidance literature:: Multi-step reaction with 8 steps

1: N,N-dimethyl-formamide / 5 h / 50 °C

2: hydrogenchloride / methanol / 20 °C

3: hydrogenchloride; iron / water; methanol / 20 °C

4: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C

5: chlorosulfonic acid / 2 h / 0 - 20 °C / Neat (no solvent)

6: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

7: sodium hydroxide; water / methanol / 16 h / 20 °C

8: sulfuric acid / 48 h / Reflux

With 4-methyl-morpholine; 2,6-dimethylpyridine; hydrogenchloride; chlorosulfonic acid; water; iron; sodium hydroxide; sulfuric acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 52913-11-8
(3-amino-phenyl)-acetic acid methyl ester

: 1308254-99-0
isopropyl 2-(5-amino-2-(N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)sulfamoyl)phenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C

2: chlorosulfonic acid / 2 h / 0 - 20 °C / Neat (no solvent)

3: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

4: sodium hydroxide; water / methanol / 16 h / 20 °C

5: sulfuric acid / 48 h / Reflux

With 4-methyl-morpholine; 2,6-dimethylpyridine; chlorosulfonic acid; water; sodium hydroxide; sulfuric acid; In methanol; dichloromethane; acetonitrile;