N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

Base Information

Chemical Name:N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide
CAS No.:1239365-36-6
Molecular Formula:C₁₄H₂₁N₄PSe
Molecular Weight:355.281
Hs Code.:

Synonyms:N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

Suppliers and Price of N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

Chemical Property:

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Technology Process of N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

There total 4 articles about N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1239365-28-6
4⁽⁵⁾-[bis(dimethylamino)phosphoroselenoyl]-1,3-dimethyl-2-phenyl-1H-imidazolium chloride

: 1239365-16-2
N,N,N',N'-tetramethyl-P-[1-methyl-2-phenyl-1H-imidazol-5-yl]phosphonoselenoic diamide

: 1239365-36-6
N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

Guidance literature:: at 210 - 220 ℃; under 12 Torr;
DOI:10.1002/hc.20584

Reference yield:

: 1227185-99-0
N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide

: 1239365-36-6
N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

Guidance literature:: Multi-step reaction with 3 steps

1: selenium / benzene / 20 °C / Inert atmosphere

2: 6 h / 70 - 75 °C / sealed tube

3: 210 - 220 °C / 12 Torr

With selenium; In benzene;
DOI:10.1002/hc.20584

Reference yield:

: 1227185-86-5
1-methyl-2-phenyl-1-H-imidazol-5-yl-phosphonous dichloride

: 1239365-36-6
N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-4-yl)phosphonoselenoic diamide

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / -30 - 20 °C / Inert atmosphere

2: selenium / benzene / 20 °C / Inert atmosphere

3: 6 h / 70 - 75 °C / sealed tube

4: 210 - 220 °C / 12 Torr

With selenium; In diethyl ether; benzene;
DOI:10.1002/hc.20584