N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide

Base Information

• Chemical Name: N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide
• CAS No.: 1227185-99-0
• Molecular Formula: C₁₄H₂₁N₄P
• Molecular Weight: 276.321

Synonyms:N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide

Chemical Property of N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide

Chemical Property:

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Technology Process of N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide

There total 2 articles about N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-methyl-2-phenyl-1-H-imidazol-5-yl-phosphonous dichloride (1227185-86-5) + dimethyl amine (124-40-3) → N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide (1227185-99-0)

Guidance literature:

In diethyl ether; at -30 - 20 ℃; Inert atmosphere;

DOI:10.1002/hc.20584

Reference yield: 75.0%

1-methyl-2-phenyl-1H-imidazol-5-yl-phosphonous dibromide (1227185-88-7) + dimethyl amine (124-40-3) → N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide (1227185-99-0)

Guidance literature:

In benzene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/hc.20550

Reference yield: 92.0%

N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide (1227185-99-0) → N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonic diamide (1239365-11-7)

Guidance literature:

N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide; With hexachloroethane; In dichloromethane; at 0 - 5 ℃; for 0.5h; Inert atmosphere;

With triethylamine; In dichloromethane; Inert atmosphere;

With water; In dichloromethane; at 0 - 5 ℃; Inert atmosphere;

DOI:10.1002/hc.20584

upstream raw materials:

1-methyl-2-phenyl-1H-imidazol-5-yl-phosphonous dibromide

dimethyl amine

1-methyl-2-phenyl-1-H-imidazol-5-yl-phosphonous dichloride

Downstream raw materials:

C₁₄H₂₁N₄PS

N,N,N',N'-tetramethyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonic diamide

N,N,N',N'-tetramethyl-P-[1-methyl-2-phenyl-1H-imidazol-5-yl]phosphonoselenoic diamide

4⁽⁵⁾-[bis(dimethylamino)phosphinyl]-1,3-dimethyl-2-phenyl-1H-imidazolium chloride

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